GCMS blank analysis results for sample AE00110, Feb 2002

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Data File : C:\MSDCHEM\l\5973N\02FEB04\0204BB.D Vial: 1 . Acq On : 4 Feb 2002 10:58 am Operator: Sample : lab blank l/4b Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C: \MSDCHEM\1 . . . \SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 12 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.36 ug/L 256993 Phenanthrene-dl0 22.65 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 87 2 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 83 3 Anthracene-D10 188 C14D10 000000-00-0 64 4 anti-10-hydroxy-5,6,8,9-tetrahyd... 188 C12H1202 055139-53-2 50 Abundance Scan 1699 (22.771 min): 0204BB.D (-) m/z 188.15 100.00% 1118

5000

94 114411IIT MIT |- 1 > । i i r-t ■ [ i ■ 80 199 158 i 22.40 22.60 22.80 23.00 23.20

mtz~> 44 54 Of -PTHTITH 40 50 60 70 80 66 -*H 90 100 110 120 130 140 150 160 170 180 190 m/z 94.10 17.25% Abundance #84499: Phenanthrene-d10 188

5000 m 22.40 22.60 22.80 23.00 23.20 80 m/z 184.10 14.07% 160

yJz~> 0 TmTTT - 66 94

40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 -l Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 80.10 10.99%

80 94 66 158 . 0 LWTPTTTTTTT TTTTf TITMMI > । i i . r p > i 11 > i . > । i . ri । i . I b| i i i ■ । > > .. ] > ’ll 1nur miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 ■ i ■ ■ ■ ■ i ■ ■ ' 1 i • 1 ■ ■ i ■ ■ • ‘ i ■ 188 22.40 22.60 22.80 23.00 23.20 m/z 189.15 10.18%

5000 80 94 66 160 - 0- “ i" " i • ‘ 11" -rp-r ‘ T mmmmmmmmH miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

J204BB.D SCAN508.M Tue Feb 05 09:47:47 2002 Page 14

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