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← Document results/DEP Box 28/GCMS X 1/4/02 A 1/24 - 1/25/02
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GCMS analysis results for sample AE00167, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050481–000050499

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) Data File : C:\MSDCHEM\l\5973N\02JAN24\00167.D Vial: 4 * Acq On : 24 Jan 2002 2:09 pm Operator: ■Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 25 10:22:02 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 9.72 152 1697266 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 7167974, 20.00 ug/L -0.02 17) Acenaphthene-dl0 18.34 164 3645125 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 5957986 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 5077750 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 3693450 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD 27.73 235 374690 3.98 ug/L 0.00 Spiked Amount 5.000 Recovery = 79.60% Target Compounds Qvalue 20) Dimethylphthalate 18.34 163 578772 2.40 ug/L + 56 21) 2,6-Dinitrotoluene 18.34 165 466460 9.93 ug/L # 17 42) Bis(2-ethylhexyl)phthalate 31.11 149 12801 0.60 ug/L # 65

(#) = qualifier out of range (m) = manual integration 00167.D SCAN508.M Fri Jan 25 10:22:03 2002 Page 1

NYC-WTC_000050483

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NYC-WTC_000050483Source: NYC Law Department, mirrored locally

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