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GCMS analysis results for sample AE00247, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050539–000050557

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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Scanned page image, NYC-WTC_000050541
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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data’ File : C:\MSDCHEM\1\5973N\02JAN24\00247.D Vial: 3 * Acq 'On : 24 Jan 2002 4:38 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 25 10:22:06 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 1644191 20.00 ug/L 0.00 10) Naphthalene-d8 13.20 136 6925841' 20.00 ug/L -0.01 17) Acenaphthene-diO 18.34 164 3499860 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 5562797 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 4811523 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 3551847 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 307010 3.49 ug/L 0.00 Spiked Amount 5.000 Recovery = 69.80% Target Compounds Qvalue 20) Dimethylphthalate 18.34 163 554540 2.40 ug/L # 56 21) 2,6-Dinitrotoluene 18.34 165 441952 9.80 ug/L # 17 42) Bis(2-ethylhexyl)phthalate 31.11 149 20410 0.63 ug/L 98

(#) = qualifier out of range (m) = manual integration 00247.D SCAN508.M Fri Jan 25 10:22:07 2002 Page 1

NYC-WTC_000050541

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NYC-WTC_000050541Source: NYC Law Department, mirrored locally

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