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GCMS analysis results for sample AE00168, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00168 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050500–000050518

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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Scanned page image, NYC-WTC_000050502
OCR text

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File : C:\MSDCHEM\1\5973N\02JAN24\00168.D Vial: 1 * Acq On : 24 Jan 2002 2:59 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 25 10:22:03 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1. . .\SCAN5 08. M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 9.72 152 1491818 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 6431583 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 3332964 20.00 ug/L -0.01 29) Phenanthrene-diO 22.65 188 5447319 20.00 ug/L -0.02 38) Chrysene-dl 2 30.50 240 4440597 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 3175060 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 301692 3.50 ug/L 0.00 Spiked Amount 5.000 Recovery = 70.00% Target Compounds Qvalue 20) Dimethylphthalate 18.34 163 533948 2.43 ug/L + 56 21) 2,6-Dinitrotoluene 18.34 165 416775 9.71 ug/L # 17 42) Bis(2-ethylhexyl)phthalate 31.11 149 10370 0.60 ug/L 81

(#) = qualifier out of range (m) = manual integration 00168.D SCAN508.M Fri Jan 25 10:22:04 2002 Page 1

NYC-WTC_000050502

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NYC-WTC_000050502Source: NYC Law Department, mirrored locally

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