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Document / 18 pages

GCMS analysis results for sample AD31674, Jan 25 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050276–000050293

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) Data File : C: \MSDCHEM\1\5973N\02JAN22\31674 . D Vial: 2 Acq On : 22 Jan 2002 3:30 pm Operator: 'Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 22 16:54:54 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.71 152 1457060 20.00 ug/L -0.01 10) Naphthalene-d8 13.19 136 6171125 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 3165496 20.00 ug/L -0.01 2 9) Phenanthrene-dl0 22.65 188 5111830 20.00 ug/L -0.02 38) Chrysene-dl2 30.50 240 4277893 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 2986899 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 399196 4.94 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.80% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.60 74 16164 0.26 ug/L + 16 20) Dimethylphthalate 18.34 163 506305 2.42 ug/L + 56 21) 2,6-Dinitrotoluene 18.34 165 403780 9.90 ug/L # 17 35) Di-n-butylphthalate 24.86 149 220169 0.67 ug/L 100 42) Bis(2-ethylhexyl)phthalate 31.11 149 10209 0.60 ug/L 99

(#) = qualifier out of range (m) = manual integration 31674.D SCAN508.M Tue Jan 22 16:54:54 2002 Page 1

NYC-WTC_000050278

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NYC-WTC_000050278Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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