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GCMS analysis results for sample AD31647, Jan 25 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31647 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050205–000050221

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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Scanned page image, NYC-WTC_000050207
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\MSDCHEM\1\5973N\02JAN22\31647.D Vial: 3 Acq Ori : 22 Jan 2002 1:51 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 22 15:30:27 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 •Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 9.71 152 1065496 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 4521952 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2418589 20.00 ug/L -0.01 2 9) Phenanthrene-dl0 22.63 188 4135210 20.00 ug/L -0.03 38) Chrysene-dl2 30.49 240 3516767 20.00 ug/L -0.02 44) Perylene-dl2 34.42 264 2512593 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 297132 4.55 ug/L 0.00 Spiked Amount 5.000 Recovery = 91.00% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.60 74 12189 0.27 ug/L + 13 20) Dimethylphthalate 18.34 163 386553 2.42 ug/L + 55 21) 2,6-Dinitrotoluene 18.34 165 306496 9.84 ug/L # 17 35) Di-n-butylphthalate 24.85 149 111555 0.42 ug/L 98 42) Bis(2-ethylhexyl)phthalate 31.09 149 11944 0.62 ug/L 89

(#) = qualifier out of range (m) = manual integration 31647.D SCAN508.M Tue Jan 22 15:30:28 2002 Page 1

NYC-WTC_000050207

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NYC-WTC_000050207Source: NYC Law Department, mirrored locally

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