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GCMS analysis results for sample AD31646, Jan 25 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31646 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050240–000050257

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) . Data File : C:\MSDCHEM\1\5973N\O2JAN22\31646.D Vial: 2 Acq On : 22 Jan 2002 1:02 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multipir: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 22 15:30:25 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 9.71 152 1119920 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 4690962 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2415640 20.00 ug/L -0.01 29) Phenanthrene-diO 22.63 188 3999290 20.00 ug/L -0.03 38) Chrysene-dl2 30.49 240 3561109 20.00 ug/L -0.02 44) Perylene-d12 34.42 264 2637257 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 294092 4.65 ug/L 0.00 Spiked Amount 5.000 Recovery = 93.00% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.60 74 14312 0.30 ug/L + 13 20) Dimethylphthalate 18.34 163 385086 2.41 ug/L + 55 21) 2,6-Dinitrotoluene 18.34 165 304935 9.80 ug/L # 17 35) Di-n-butylphthalate 24.85 149 129755 0.50 ug/L 100 42) Bis(2-ethylhexyl)phthalate 31.11 149 7582 0.59 ug/L 100

(#) = qualifier out of range (m) = manual integration 31646.D SCAN508.M Tue Jan 22 15:30:26 2002 Page 1

NYC-WTC_000050242

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NYC-WTC_000050242Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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