GCMS analysis results for sample AE00107, Feb 13 2002

NYC 9/11 Public Portal Document

Library Search Compound Report 8 Data File : C:\HPCHEM\1\DATA\JAN2402\107.D Vial: 14 Acq On : 25 Jan 2002 1:49 am Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.43 3.42 ug/1 913026 1,4-Dichlorobenzene-d4 11.48

Hit#.of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 4 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 5 Abundance Scan 260 (7.434 min): 107.D (-) m/z 73.00 100.00% 73

5000- 43 -n-j-r-T-r

87 103 7.00 7.20 7.40 7.60 7.80 i 38 I, | 50 5,5. .61 67, , IP ! i ' ■ ■ ' i ' 1 ' ■ । 1 1 ‘ I 1 1 ' ' i ■ ' ■ ■ i ' ' ■ ■ I m/ z 43.0.0 32.36% m/z-> 10 20 30 40 50 60 70 80 90 100 110 [Abundance #62932: Silane, tetramethyl- 73

5000 7.00 7.20 7.40 7.60 7.80 45 m/z 41.00 11.62% 15. | 53 59 1 88 -j i‘i-i-i-1 j । . miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292; N-Ethylformamide 30 73 "I T I i i । T I I i | । i-i i । COm"rr r i 7.00 7.20 7.40 7.60 7.80 5000- m/z 44.9.5 11.48% 44 58

15 IIIII1IIIIIII**G . : n/z-> 10 20 30 40 50 60 70 80 90 100 110 'Abundance #1761: Butane, 2-methoxy-2-methyl- 73 7.00 7.20 7.40 7.60 7.80 m/z 71.00 6.64% 5000 55 87 45 2/ 33 I _.......... 1 . i ' ' ■ ■ i ' ' ■ ■ i ' ' ' ' i i ■ • • ■ i ■ • " ■ r■ 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.00 7.20 7.40 7.60 7.80

107.D GCMS0208.M Fri Feb 08 13:38:55 2002 Page 1

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