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GCMS analysis results for sample AD31637, Jan 28 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD31637 including unknown compounds and surrogate recovery data.

NYC-WTC_000049929–000049943

Folder label: “GCMS X 1/3/02 A 1/17/02

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Scanned page image, NYC-WTC_000049942
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library aearen compound Report

Data File : C:\MSDCHEM\1\5973N\O2 JAN17\31637.D Vial: 4 * Acq On : 17 Jan 2002 12:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1.. .\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.23 ug/L 135752 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Anthracene-dlO- 188 C14D10 001719-06-8 91 2 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 3 Anthracene-D10 188 C14D10 000000-00-0 91 4 Phenanthrene-dl0 188 C14D10 001517-22-2 91 Abundance Scan 1699 (22.771 min): 31637.D (-) m/z 188.10 100.00% 110

5000

80 94 . "I8 • • i • • • ■ । > 160 22.40 22.60 22.80 23.00 23.20 40 52 66 — > > । > 11! 1111 ■ i ■ 11111111 > 111 ■ 111111111111111111111111 0- ■ ■ i" ‘ ■ i1 ■1 IP TTT m/z 189.10 16.94% niz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- 110

1 • 5000 22.40 22.60 22.80 23.00 23.20 m/z 94.10 15.96% 66 80 94 160 , I

miz-> oR “ i ■ ■ ‘' i ■ -9 ----- 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Wt

Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 80.10 14.73%

80 94 66 158 Of ■' I'11111 ■" I''1' l''' ■ ttttT — sallanas niz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 ......... ............... ... 110 22.40 22.60 22.80 23.00 23.20 m/z 184.10 14.48%

5000

80 94 66 160 । - 0i i “ ■ ■ i -H ‘ I 1-rrrT m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

31637.D SCAN508.M Tue Jan 22 08:36:59 2002 Page 10

NYC-WTC_000049942

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NYC-WTC_000049942Source: NYC Law Department, mirrored locally

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