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GCMS analysis results for sample AE00465, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00465 conducted on January 18, 2002.

NYC-WTC_000051222–000051235

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051233
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN10\00328.D Vial: 1 Acq On : 10 Jan 2002 2:49 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Muitiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 6 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.52 ug/L 283171 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 95 2 Anthracene-DlO 188 C14D10 000000-00-0 91 3 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 4 Phenanthrene-dlO 188 C14D10 001517-22-2 90 Abundance Scan 1699 (22.771 min): 00328.D (-) m/z 188.20 100.00% 188 1)

5000

"IT T’ ’ 1 'I ' 1 1 1 1 1 52 < l • 66 80 94 1 60 —— • (• l > ■1111 ■ • (11 ■ vp ।।। 11111111111111111111'| 111 22.40 22.60 22.80 23.00 23.20 01 TT m/z 94.05 14.62% n/z-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d IQ- 188

5000 'I 1 1 1 r 1 r IT 22.40 22.60 22.80 23.00 23.20 m/z 189.10 12.30% __ 80 94 160

mlz-> 0 a50 60 66 70 I 80 I । ■ ■ ■ ■ । • ■' > । ■ ■ ■ ■ । 90 100 110 120 130 140 150 160 170 180 190 —

Abundance #84498: Anthracene-D10 188

22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 11.56% 80 11 94 66 160 o1 - - i ■ ■ 111'~, ■ 'r- i' '' ' i' ■ '' i '' ' ' i mfe-> 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 ............ .............. ..................... 188 22.40 22.60 22.80 23.00 23.20 m/z 80.00 10.08% 5000

80 94 66 158 —— miz-> 0 TTTT TIT 50 60 70 80 —TmTIIHTT 90 100 110 120 130 140 150 160 170 180 190 0 2240 22.60 22.80 23.00 23.20

)0328.D SCAN508.M Fri Jan IT 10:08:22 2002 Page 8

NYC-WTC_000051233

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NYC-WTC_000051233Source: NYC Law Department, mirrored locally

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