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GCMS reference results for sample AD29228, January 2002

Machine-extracted title · confidence 100%

Reference analysis report for GCMS testing of sample AD29228 conducted on January 4, 2002.

NYC-WTC_000049787–000049794

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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Scanned page image, NYC-WTC_000049791
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NYC 9/11 Public Portal Document

LSC Area Percent Report

* Data File C:\HPCHEM\1\DATA\JANO3O2\LB.D Vial: 18 Acq On 4 Jan 2002 3:08 am Operator: 209 GALOS Sample gems scan 1/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.465 260 264 296 rBV 416653 1234942 20.38% 4.131% 2 11.523 701 706 730 rBV 1834497 4714603 77.79% 15.769% 3 15.122 1092 1098 1117 rBV 2859453 5937866 97.97% 19.861% 4 20.391 1666 1672 1693 rBV 2927066 6060948 100.00% 20.272% 5 24.807 2146 2153 2164 rBV2 2543489 5493923 90.64% 18.376%

6 24.954 2166 2169 2188 rVB2 16839 62989 1.04% 0.211% 7 29.884 2701 2706 2714 rBV 350966 670682 11.07% 2.243% 8 32.831 3020 3027 3044 rBV2 1519217 3448045 56.89% 11.533% 9 36.898 3463 3470 3485 rBV 876702 2273699 37.51% 7.605%

Sum of corrected areas: 29897697

LB.D GCMS0103.M Fri Jan 11 08:34:22 2002

NYC-WTC_000049791

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NYC-WTC_000049791Source: NYC Law Department, mirrored locally

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