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GCMS analysis results for sample AD29292, Jan 22 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD29292 including unknown compounds and surrogate recovery data.

NYC-WTC_000049823–000049832

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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Scanned page image, NYC-WTC_000049828
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\JAN03 02\2 92 92.D Vial: 23 Acq On 4 Jan 2002 7:58 am Operator: 209 GALOS Sample gems scan 1/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.467 260 264 276 rBV 225530 620350 12.11% 2.507% 2 7.605 277 279 297 rVB 27977 111315 2.17% 0.450% 3 11.525 701 706 727 rBV 1494891 3906740 76.27% 15.790% . 4 15.123 1092 1098 1117 rBV 2342467 4987949 97.38% 20.160% 5 20.384 1665 1671 1698 rBV 2436730 5122402 100.00% 20.704%

6 24.800 2146 2152 2165 rBV2 2235924 4674558 91.26% 18.893% 7 29.885 2706 2706 2715 rBV 246609 486485 9.50% 1.966% 8 32.832 3021 3027 3041 rBV2 1281961 2912394 56.86% 11.771% 9 36.899 3463 3470 3484 rBV 709621 1919514 37.47% 7.758%

Sum of corrected areas: 24741707

29292.D GCMS0103.M Fri Jan 11 08:30:13 2002

NYC-WTC_000049828

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NYC-WTC_000049828Source: NYC Law Department, mirrored locally

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