GCMS analysis results for sample AE08962, May 7, 2002

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Data File : C:\MSDCHEM\1\DATA\020424\08962.D Vial: 13 Acq On : 24 Apr 2002 9:39 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.12 0.63 ug/1 714688 1,4-Dichlorobenzene-d4 11.38

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 50 2 2-Propanone, 1,1-di chioro- 126 C3H4C120 000513-88-2 25 3 3-Oxobutyric acid, 2-chloroethyl... 164 C6H9C1O3 1000210-13-3 9 4 1-Fluorononane______________________ 146 C9H19F 000463-18-3 9 Abundance Scan 518 (6.123 min): 08962.D (-512) (-) m/ z 43.10 100.00% 43

5000 ________ N — _____ »»»|<»»» । > i » I J-1 i » » | r i i i ।

35 " i" " i1 ■" i ■ ■ ,52 63 83 97.... 1171f............... 3rmmun । .... ।. ...... ’ b . ’ ’1 . i n ।.. i. ।. . . i । .. i ( i . 5.80 m/z 125.00 6.00 6.20 6.40 9.35% niz-> 10 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 Abundance #3877:2-Propanone, 1,1,1 -trichloro- 43

5000 / • • • i • • » • i > • • WWAA • T■ . i . । । 5.80 6.00 6.20 6.40 m/z 97.00 5.31% 15

mfa-> 4 ,27,,35,++453.453.,73..33+87 27 35 — .117125, 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 »»i *11 ‘ i ‘ • i' “11 * •

Abundance #3861:2-Propanone, 1,1 -dichloro- 43 ------ 5.80 6.00 6.20 6.40 5000 m/z 126.90 5.15%

15 27

mk-> — ml**++1— 35 63 83 93 125 rpttp’h 1’, 1। ’’11E3111111091 ’—33T—E3’T"T"IUTTIET 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #7067:3-Oxobutyric acid, 2-chloroethyl ester --------------------- 43 5,80 6.00 6.20 6.40 m/z 83.00 4.76%

5000-

63 _ 85 514473.93,102 115 124 136 149 164 111 i1 ■ " i ■ ■" i1 ‘1 ■ i" ■ ■ i ■' “ i ■ ■ er. AACMm, । । i'i । MMAM, m 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 5.80 6.00 6.20 6.40

08962.D SCAN020424.M Thu May 02 14:47:53 2002 Page 5

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