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GCMS analysis results for sample AE08962, May 7, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08962 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049596–000049608

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document UV ALSa rCLWILL RSDULU

Data File : C:\MSDCHEM\1\DATA\020424\08962.D Vial: 13 Acq On : 24 Apr 2002 9:39 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 5 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.349 42 46 51 W 4 30066 384849 0.54% 0.102% 2 3.649 92 97 107 VB 37650 534410 0.75% 0.141% 3 6.123 512 518 520 PV 48940 714688 1.01% 0.189% 4 6.158 520 524 560 W 679985 14326589 20.16% 3.790% 5 11.375 1400 1412 1432 PV 1775663 45347559 63.80% 11.996% 6 16.534 2277 2290 2312 PV 2468243 62587947 88.06% 16.557% 7 24.460 3617 3639 3653 PV 2633918 71075339 100.00% 18.802% 8 27.539 4151 4163 4177 W 3 283434 7545201 10.62% 1.996% 9 31.088 4752 4767 4780 PV 4 18325 559536 0.79% 0.148% 10 31.717 4854 4874 4891 W 2 2399744 69509878 97.80% 18.388% 11 31.958 4908 4915 4929 W 3 21711 626302 0.88% 0.166% 12 39.931 6260 6272 6294 BV 2 3146153 59102591 83.15% 15.635% 13 43.156 6808 6821 6838 PV 2 2441152 45707589 64.31% 12.091%

Sum of corrected areas: 378022479

08962.D SCAN020424.M Thu May 02 14:47:47 2002 Page 1

NYC-WTC_000049600

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NYC-WTC_000049600Source: NYC Law Department, mirrored locally

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