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GCMS analysis results for sample AE10025, May 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE10025 conducted on May 14, 2002, identifying unknown compounds.

NYC-WTC_000044191–000044202

Folder label: “GCMS X 4/26/02 A 5/8/02

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NYC 9/11 Public Portal Document

' Data File C:\MSDCHEM\l\DATA\020507\10025.D Vial: 24 Acq On 8 May 2002 10:47 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.7 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.012 323 329 346 rBV 129613 219311 4.37% 0.757% 2 5.800 458 463 478 rVB2 88257 165591 3.30% 0.572% 3 6.152 513 523 560 rBV 651377 1352395 26.95% 4.668% 4 11.376 1399 1412 1429 rBV 1385441 3580301 71.34% 12.358% 5 16.534 2276 2290 2308 rBV 1737487 4478411 89.23% 15.458%

6 24.461 3620 3639 3651 rBV 1721670 4671653 93.08% 16.125% 7 27.533 4149 4162 4176 rBV4 246372 683348 13.62% 2.359% 8 31.076 4759 4765 4778 rBV5 11716 36290 0.72% 0.125% 9 31.717 4858 4874 4891 rBV2 1668514 5018828 100.00% 17.324% 10 31.952 4906 4914 4923 rBV2 16147 43989 0.88% 0.152%

11 39.931 6261 6272 6293 rBV2 2241349 4581629 91.29% 15.814% 12 40.518 6365 6372 6394 rVB2 206439 466358 9.29% 1.610% 13 43.157 6807 6821 6844 rBV 1773368 3673030 73.19% 12.678%

Sum of corrected areas: 28971134

10025.D SCAN020507.M Tue May 14 08:46:10 2002 Page 1

NYC-WTC_000044195

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NYC-WTC_000044195Source: NYC Law Department, mirrored locally

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