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GCMS analysis results for sample AE10208, May 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of sample AE10208 conducted on May 20, 2002, including surrogate recovery data.

NYC-WTC_000024319–000024332

Folder label: “GCMS X 5/1/02 A 5/9/02

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Scanned page image, NYC-WTC_000024323
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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\020509\10208.D Vial: 10 Acq On 9 May 2002 7:31 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.7 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total.

1 6.152 514 523 564 rBV 735442 1514230 24.26% 4.418% 2 11.375 1400 1412 1434 rBV 1734688 4431657 70.99% 12.930% 3 16.534 2275 2290 2313 rBV 2004193 5617549 89.99% 16.391% 4 24.460 3618 3639 3659 rBV 1971349 5839060 93.54% 17.037% 5 27.539 4147 4163 4177 rBV4 285096 807667 12.94% 2.357%

6 31.088 4756 4767 4782 rBV4 15435 50112 0.80% 0.146% 7 31.723 4855 4875 4899 rBV2 1957615 6242618 100.00% 18.214% 8 31.952 4906 4914 4923 rVB3 18598 49344 0.79% 0.144% 9 33.832 5223 5234 5244 rBV 31273 78785 1.26% 0.230% 10 36.505 5679 5689 5699 rBV 48336 111622 1.79% 0.326%

11 38.591 6031 6044 6057 rBV 35282 91039 1.46% 0.266% 12 39.937 6259 6273 6301 rBV2 2603274 5391722 86.37% 15.732% 13 40.524 6366 6373 6390 rVB5 15653 46445 0.74% 0.136% 14 43.156 6807 6821 6841 rBV2 1913225 4001057 64.09% 11.674%

Sum of corrected areas: 34272907

10208.D SCAN020507.M Tue May 14 14:22:24 2002 Page 1

NYC-WTC_000024323

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NYC-WTC_000024323Source: NYC Law Department, mirrored locally

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