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GCMS analysis results for sample AE10067, May 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE10067 conducted on May 14, 2002, including surrogate recovery data.

NYC-WTC_000044227–000044238

Folder label: “GCMS X 4/26/02 A 5/8/02

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Scanned page image, NYC-WTC_000044231
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NYC 9/11 Public Portal Document

Data File C: \MSDCHEM\1\DATA\020507\10067.D Vial: 27 Acq On 8 May 2002 1:44 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.7 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 6.123 511 518 519 rBV 26171 39978 0.77% 0.137% 2 6.152 519 523 563 rVB 660261 1347345 25.82% 4.629% 3 9.331 1061 1064 1079 rBV8 11903 39230 0.75% 0.135% 4 11.375 1399 1412 1433 rBV 1441984 3731664 71.51% 12.822% 5 16.534 2276 2290 2313 rBV 1768223 4705543 90.17% 16.168%

6 24.460 3622 3639 3650 rBV2 1775426 4877791 93.47% 16.759% 7 27.533 4143 4162 4174 rBV4 260718 736107 14.11% 2.529% 8 31.088 4757 4767 4778 rVB4 13175 41503 0.80% 0.143% 9 31.723 4853 4875 4896 rBV2 1708560 5218580 100.00% 17.930% 10 31.952 4902 4914 4922 rBV5 17179 48001 0.92% 0.165%

11 34.801 5390 5399 5409 rBV2 17537 42261 0.81% 0.145% 12 39.931 6260 6272 6296 rBV2 2378865 4659206 89.28% 16.008% 13 40.524 6364 6373 6390 rVB2 57846 153011 2.93% 0.526% 14 43.151 6808 6820 6838 rBV2 1664801 3464509 66.39% 11.904%

Sum of corrected areas: 29104729

10067.D SCAN020507.M Tue May 14 08:47:15 2002 Page 1

NYC-WTC_000044231

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NYC-WTC_000044231Source: NYC Law Department, mirrored locally

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