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GCMS analysis results for sample AEO8O6S, May 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AEO8O6S performed on May 7, 2002, including detection of unknown compounds.

NYC-WTC_000049547–000049558

Folder label: “GCMS X 4/16/02 A 4/24/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020424\08958.D Vial: 9 Acq On : 24 Apr 2002 5:44 pm Operator: Nefliu Sample : sample Inst : Instrumen Misc Multiplr: 1.00 MS Integration Params: events.e Quant Time: Apr 26 09:38:13 2002 Quant Results File: SCAN020424.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Wed Apr 24 08:54:34 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Conc Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 9562456 40.00 ug/l -0.01 10) Naphthalene-d8 16.54 136 37400994 40.00 ug/l -0.03 17) Acenaphthene-d10 24.46 164 20899298 40.00 ug/l -0.02 30) Phenanthrene-d10 31.72 188 31154219 40.00 ug/l -0.02 38) Chrysene-d12 39.94 240 24786854 40.00 ug/l -0.04 44) Perylene-d12 43.16 264 16834507 40.00 ug/l -0.02 System Monitoring Compounds 27) TCMX 27.54 207 996135 8.47 ug/l -0.03 Spiked Amount 10.000 Recovery = 84.70% Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.53 149 70084 0.16 ug/l 99

-------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed 08958.D SCAN020424.M Fri Apr 26 09:42:35 2002 Page 1

NYC-WTC 000049549

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NYC-WTC_000049549Source: NYC Law Department, mirrored locally

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