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GCMS reference analysis results for sample AE08958, April-May 2002

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Laboratory report of GCMS reference analysis for sample AE08958 listing chemical standards and response values.

NYC-WTC_000049539–000049543

Folder label: “GCMS X 4/16/02 A 4/24/02

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NYC 9/11 Public Portal Document quantltatlon Keporc (V1 Keviewed)

Data File : C:\MSDCHEM\1\DATA\020424\0416REF2.D Vial: 6 Acq On : 24 Apr 2002 2:47 pm Operator: Nefliu Sample : 04/16 ref Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: events.e Quant Time: Apr 26 09:19:41 2002 Quant Results File: SCAN020424.RE Quant Method : C: \MSDCHEM\1\METHODS\SCAN020424 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Wed Apr 24 08:54:34 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoranthene 36.06 202 14593128 17.57 ug/1 99 39) Pyrene 36.66 202 15324613 19.38 ug/1 99 40) Buthylbenzylphthalate 38.93 149 6165294 17.99 ug/1 100 41) Benz(a)anthracene 39.92 228 12942151 18.26 ug/1 99 42) Chrysene 40.00 228 11949218 18.79 ug/1 100 43) Bis(2-ethylhexyl)phthalate 40.53 149 7412892 17.79 ug/1 99 45) Di-n-Octyl phthalate 42.04 149 10244974 14.98 ug/1 98 46) Benzo(b)fluoranthene 42.38 252 9590056m 17.00 ug/1 47) Benzo(k)fluoranthene 42.44 252 9772628 16.60 ug/1 100 48) Benzo(a)pyrene 43.02 252 6495788m 12.44 ug/1 49) Indeno(l,2,3-cd)pyrene 45.22 138 1937274 13.89 ug/1 97 5 0) Dibenz(a,h)anthracene 45.32 139 1676192 16.95 ug/1 97 51) Benzo(ghi)perylene 45.77 276 5661260 17.24 ug/1 97

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0416REF2.D SCAN020424.M Fri Apr 26 09:27:10 2002 Page 2

NYC-WTC_000049542

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NYC-WTC_000049542Source: NYC Law Department, mirrored locally

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