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GCMS reference standard results, May 2002

Machine-extracted title · confidence 100%

Laboratory record of reference standard analysis for volatile organic compounds using GCMS methods from May 13 to May 15, 2002.

NYC-WTC_000024441–000024449

Folder label: “GCMS X 5/13/02 A 5/16/02

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NYC 9/11 Public Portal Document quantitatlon Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020515\0513REF3.D Vial: 7 Acq On : 15 May 2002 5:45 pm Operator: Nefliu Sample : 05/13 ref Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 16 14:50:00 2002 Quant Results File: SCAN020507 .RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 16 14:49:15 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoranthene 36.05 202 694227 17.08 ug/1 97 3 9) Pyrene 36.66 202 737527 18.80 ug/1 97 40) Buthylbenzylphthalate 38.93 149 321591 17.04 ug/1 95 41) Benz(a)anthracene 39.92 228 592512 17.04 ug/1 99 42) Chrysene 39.99 228 587667 17.95 ug/1 99 43) Bis(2-ethylhexyl)phthalate 40.52 149 529870 22.05 ug/1 95 45) Di-n-Octyl phthalate 42.03 149 531048 14.46 ug/1 99 46) Benzo(b)fluoranthene 42.37 252 454988 17.39 ug/1 98 47) Benzo(k)fluoranthene 42.43 252 480177 17.94 ug/1 98 48) Benzo(a)pyrene 43.02 252 328753 13.11 ug/1 96 49) Indeno(1,2,3-cd)pyrene 45.22 276 216347 11.66 ug/1 97 50) Dibenz(a,h)anthracene 45.32 278 240852 13.69 ug/1 96 51) Benzo(ghi)perylene 45.77 276 264784 14.89 ug/1 96

\

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0513REF3.D SCAN020507.M Thu May 16 14:50:39 2002 Page 2

NYC-WTC_000024445

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NYC-WTC_000024445Source: NYC Law Department, mirrored locally

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