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GCMS analysis results, sample AE08956, April 2002

Machine-extracted title · confidence 80%

Gas chromatography-mass spectrometry analysis of environmental sample AE08956 conducted on April 29, 2002, detecting unknown compounds and 2,4-DDD surrogate at 79 micrograms.

NYC-WTC_000049288–000049298

Folder label: “GCMS X 4/15/02 A 4/22/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\042202\8956.D Vial: 18 Acq On : 23 Apr 2002 1:06 am Operator: Bohlk Sample : SAMPLE 8956 4/15/02, FB Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Toluene Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

3.88 6.87 ug/L 544186 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Toluene 92 C7H8 000108-88-3 95 2 Toluene 92 C7H8 000108-88-3 91 3 Toluene 92 C7H8 000108-88-3 91 4 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 91 Abundance Scan 137 (3,884 min): 8956.D (-) m/z 91.10 100.00%l 91

5000

65 3.60 3.80 4.00 4.20” 39 AR 51 |

miz-> 0- . ............... 0 1 35,44... 1 1/78-1185171 10 20 30 40 50 60 70 80 90 100 m/z 92.10 58.12%

Abundance #5541: Toluene 91

5000 T T T T 3.60 3.80 4.00 4.20 m/z 65.10 14.14 39 51 65 Tl/Z-> 0- • ■ i ■ • 1 ■ i • • ■ ■ i ■ ■ 0 10 20 27 30 i • +457157, 40 L 50 60 TIT 70 77 80 851190 100 Abundance #5542: Toluene 91

11111 4 3.60 3.80 4.00 4.20 5000 m/z39.10 8.17

39 27 45 51 65 77 85 „ 0- " 11''11111111''11111 Trt ril nlr '' ill ' i ■ TTTTT I

m/z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #5538: Toluene 91 3.60 3.80 4.00 4.20 m/z63.10 8.09

5000

39 45 51 65 ? - 11

m/z—> 0- 1 15 27 . ■ i‘‘ ■ ■' i1 ' • ■ i ■ - 0 10 20 30 — 40 57 50 60 70 77 85 । I' 80 I 90 100 •1 'i1 u 3.60 3.80 4.00 4.20

8956.D 5080402BBC.M Fri Apr 26 12:16:24 2002 Page 3

NYC-WTC_000049295

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NYC-WTC_000049295Source: NYC Law Department, mirrored locally

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