GCMS analysis results, Sample AE08267, April 22, 2002

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GCMS analysis report for sample AE08267 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048421–000048435

Folder label: “GCMS X 4/9/02 A 4/17/02”

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NYC 9/11 Public Portal Document

.38 13.638 1789 1797 1804 W 3 10485 209164 0.30% 0.056% 39 13.878 1829 1838 1841 PV 4 2494 41157 0.06% 0.011% 40 14.754 1984 1987 1989 PV 2 1716 15735 0.02% 0.004%

41 14.848 2001 2003 2008 PV 1670 28478 0.04% 0.008% 42 15.300 2072 2080 2091 W 3 5395 118305 0.17% 0.032% 43 15.571 2122 2126 2137 W 4 2626 75519 0.11% 0.020% 44 15.753 2152 2157 2163 W 4 4048 87165 0.12% 0.023% 45 16.799 2324 2335 2352 W 3 7347 194648 0.28% 0.052%

46 17.216 2394 2406 2408 W 3 2083 67470 0.10% 0.018% 47 17.280 2412 2417 2423 W 2 2164 51084 0.07% 0.014% 48 17.445 2440 2445 2450 W 2 2273 52558 0.07% 0.014% 49 17.927 2525 2527 2537 PV 1674 42642 0.06% 0.011% 50 18.156 2563 2566 2573 W 2246 41975 0.06% 0.011%

51 18.632 2635 2647 2658 W 3494326 68870443 98.17% 18.552% 52 18.702 2658 2659 2664 W 5538 94628 0.13% 0.025% 53 18.738 2664 2665 2674 W 3572 93195 0.13% 0.025% 54 18.873 2685 2688 2693 W 3 3245 65300 0.09% 0.018% 55 19.020 2705 2713 2721 W 4892 129067 0.18% 0.035%

56 19.084 2721 2724 2735 W 2141 74868 0.11% 0.020% 57 19.231 2743 2749 2753 W 3 2160 60626 0.09% 0.016% 58 19.660 2817 2822 2824 W 2451 32407 0.05% 0.009% 59 19.719 2829 2832 2836 W 2382 38907 0.06% 0.010% 60 20.171 2900 2909 2911 W 2629 67332 0.10% 0.018%

61 20.206 2911 2915 2920 W 2 3940 70244 0.10% 0.019% 62 20.306 2929 2932 2934 W 2351 20205 0.03% 0.005% 63 20.389 2940 2946 2954 W 5 7517 147543 0.21% 0.040% 64 20.600 2968 2982 2990 W 353134 6272395 8.94% 1.690% 65 21.147 3072 3075 3077 W 2 2255 22622 0.03% 0.006%

66 21.452 3122 3127 3131 W 3 2278 52120 0.07% 0.014% 67 21.822 3180 3190 3194 W 3 9513 187792 0.27% 0.051% 68 21.857 3194 3196 3204 W 3 3855 88271 0.13% 0.024% 69 22.263 3260 3265 3267 W 2118 30310 0.04% 0.008% 70 22.645 3323 3330 3343 W 2 29744 573667 0.82% 0.155%

71 23.021 3382 3394 3414 W 2 3306999 70151203 100.00% 18.897% 72 23.174 3414 3420 3435 W 40101 1062575 1.51% 0.286% 73 23.285 3435 3439 3441 W 3 4766 93497 0.13% 0.025% 74 23.620 3494 3496 3498 W 2739 22866 0.03% 0.006% 75 23.644 3498 3500 3508 W 2618 73160 0.10% 0.020%

76 24.425 3628 3633 3637 W 2650 43949 0.06% 0.012% 77 25.160 3754 3758 3766 W 4 6147 152800 0.22% 0.041% 78 25.917 3881 3887 3895 PV 2 1844 61493 0.09% 0.017% 79 25.976 3895 3897 3907 W 2093 63099 0.09% 0.017% 80 27.545 4162 4164 4169 W 2425 36107 0.05% 0.010%

81 28.109 4256 4260 4265 W 2 3137 57526 0.08% ' 0.015% 82 28.350 4297 4301 4312 PV 1962 46990 0.07% 0.013% 83 29.396 4478 4479 4483 W 1735 12442 0.02% 0.003% 84 29.584 4509 4511 4516 PV 3 1416 14459 0.02% 0.004% 85 29.983 4574 4579 4582 W 3 3005 38515 0.05% 0.010%

86 30.060 4586 4592 4602 W 3 3274 92899 0.13% 0.025% 87 30.265 4625 4627 4633 PV 1733 23670 0.03% 0.006%

08267.D 041702SCAN.M Thu Apr 18 10:01:01 2002 Page 2

NYC-WTC_000048426

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NYC-WTC_000048426Source: NYC Law Department, mirrored locally

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