GCMS analysis results, Sample AE08267, April 22, 2002

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GCMS analysis report for sample AE08267 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048421–000048435

Folder label: “GCMS X 4/9/02 A 4/17/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C: \MSDCHEM\1\DATA\020417\08267.D Vial: 24 Acq On : 18 Apr 2002 4:22 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.144 3 11 20 BV 5 8074 166443 0.24% 0.045% 2 3.537 74 78 81 PV 2 1718 22422 0.03% 0.006% 3 3.579 81 85 92 W 3 3475 68446 0.10% 0.018% 4 3.737 99 112 115 PV 6 2708 75414 0.11% 0.020% 5 3.772 115 118 120 W 3 2688 45038 0.06% 0.012%

6 3.837 125 129 131 W 2 2956 45490 0.06% 0.012% 7 4.201 189 191 195 W 2 3170 40631 0.06% 0.011% 8 4.313 205 210 215 W 4 4279 97074 0.14% 0.026% 9 4.366 215 219 221 W 4 2729 40645 0.06% 0.011% 10 4.389 221 223 225 W 2 3076 34667 0.05% 0.009%

11 4.589 254 257 259 PV 2 1716 20188 0.03% 0.005% 12 4.630 259 264 268 W 4 2747 60544 0.09% 0.016% 13 4.789 285 291 295 W 6 4988 94225 0.13% 0.025% 14 4.824 295 297 299 W 2881 30339 0.04% 0.008% 15 4.883 303 307 319 W 4 6844 175596 0.25% 0.047%

16 5.065 331 338 345 W 4 4385 112673 0.16% 0.030% 17 5.159 348 354 361 W 6 3972 118782 0.17% 0.032% 18 5.318 379 381 387 PV 3 1774 31006 0.04% 0.008% 19 5.465 401 406 409 W 5 2327 49748 0.07% 0.013% 20 5.970 487 492 501 W 22633 475341 0.68% 0.128%

21 6.046 501 505 518 W 5 4705 174147 0.25% 0.047% 22 6.275 542 544 553 PV 4 2145 48827 0.07% 0.013% 23 6.704 615 617 618 W 2 2055 14417 0.02% 0.004% 24 6.828 634 638 640 W 2 1781 18039 0.03% 0.005% 25 7.703 783 787 789 W 1940 21235 0.03% 0.006%

26 7.738 789 793 795 W 1992 24521 0.03% 0.007% 27 8.491 918 921 925 W 4 2058 29664 0.04% 0.008% 28 9.055 1011 1017 1020 PV 2 1884 31922 0.05% 0.009% 29 9.642 1113 1117 1122 W 4 2607 57637 0.08% 0.016% 30 9.713 1122 1129 1134 W 6 2965 68638 0.10% 0.018%

31 9.748 1134 1135 1139 W 2158 22065 0.03% 0.006% 32 9.989 1164 1176 1189 W 2594126 47019963 67.03% 12.666% 33 10.071 1189 1190 1192 W 2 3625 36190 0.05% 0.010% 34 11.910 1497 1503 1508 PV 5 2169 48622 0.07% 0.013% 35 12.457 1582 1596 1603 W 35356 557525 0.79% 0.150%

36 13.485 1759 1771 1786 PV 3368762 62477471 89.06% 16.830% 37 13.579 1786 1787 1789 W 2 1881 18574 0.03% 0.005%

08267.D 041702SCAN.M Thu Apr 18 10:01:01 2002 Page 1

NYC-WTC_000048425

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NYC-WTC_000048425Source: NYC Law Department, mirrored locally

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