GCMS analysis results, Sample AE08265, April 22, 2002

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’88 22.557 3310 3315 3319 PV 6 2861 57534 0.09% 0.016% 89 22.592 3319 3321 3323 W 2171 20538 0.03% 0.006% 90 22.645 3323 3330 3336 W 2 28276 531602 0.80% 0.147%

91 22.709 3339 3341 3344 VV 3 2589 28640 0.04% 0.008% 92 23.021 3381 3394 3414 W 2 3144167 66835896 100.00% 18.436% 93 23.174 3414 3420 3434 W 40651 1070921 1.60% 0.295% 94 23.273 3434 3437 3444 W 5 5823 147033 0.22% 0.041% 95 23.720 3511 3513 3519 W 2 3721 73281 0.11% 0.020%

96 24.143 3576 3585 3586 W 5 2530 67578 0.10% 0.019% 97 24.178 3586 3591 3596 W 3 4272 102125 0.15% 0.028% 98 24.360 3619 3622 3625 W 2 2401 37894 0.06% 0.010% 99 24.554 3648 3655 3661 W 3305 76047 0.11% 0.021% 100 25.160 3750 3758 3766 W 5 6569 179553 0.27% 0.050%

101 25.847 3872 3875 3884 W 1935 44135 0.07% 0.012% 102 26.570 3992 3998 4007 W 3 11316 244084 0.37% 0.067% 103 26.640 4007 4010 4015 W 2088 44152 0.07% 0.012% 104 27.075 4082 4084 4086 PV 1640 13165 0.02% 0.004% 105 27.557 4158 4166 4178 W 3 1789 83854 0.13% 0.023%

106 27.645 4178 4181 4183 W 2 1924 26175 0.04% 0.007% 107 28.603 4343 4344 4348 W 2 1764 21045 0.03% 0.006% 108 28.744 4363 4368 4371 W 3 2177 39588 0.06% 0.011% 109 29.061 4419 4422 4428 W 3 2323 43139 0.06% 0.012% 110 29.120 4428 4432 4437 W 2242 39732 0.06% 0.011%

ill 29.484 4492 4494 4496 W 1715 15417 0.02% 0.004% 112 29.549 4496 4505 4512 W 3 4035 108357 0.16% 0.030% 113 29.713 4527 4533 4536 W 4 3330 63746 0.10% 0.018% 114 30.066 4580 4593 4604 W 4 4402 180539 0.27% 0.050% 115 30.295 4626 4632 4634 PV 3 1772 27234 0.04% 0.008%

116 30.583 4678 4681 4690 W 4 2062 41770 0.06% 0.012% 117 30.888 4719 4733 4761 W 2 2456014 57907746 86.64% 15.974% 118 31.059 4761 4762 4774 W 3 7625 252116 0.38% 0.070% 119 31.147 4774 4777 4780 W 3 5936 103349 0.15% 0.029% 120 31.170 4780 4781 4788 W 2 4514 98130 0.15% 0.027%

121 31.458 4822 4830 4841 W 5 11796 416772 0.62% 0.115% 122 31.529 4841 4842 4851 W 4 3540 94600 0.14% 0.026% 123 32.016 4922 4925 4926 PV 1557 11201 0.02% 0.003% 124 32.616 5022 5027 5029 W 2077 21436 0.03% 0.006% 125 32.733 5044 5047 5050 W 2089 27625 0.04% 0.008%

126 33.150 5115 5118 5121 W 3 1837 27966 0.04% 0.008% 127 34.055 5267 5272 5276 PV 3 2087 33722 0.05% 0.009% 128 34.408 5327 5332 5333 W 2 1733 26592 0.04% 0.007% 129 34.425 5333 5335 5337 W 3 2259 21904 0.03% 0.006% 130 34.684 5377 5379 5381 PV 1916 14697 0.02% 0.004%

131 34.790 5381 5397 5426 W 2 1794016 46909865 70.19% 12.940% 132 34.966 5426 5427 5435 W 6 11732 294959 0.44% 0.081% 133 35.025 5435 5437 5445 W 7 7361 239351 0.36% 0.066% 134 36.200 5632 5637 5643 W 3 3547 107808 0.16% 0.030% 135 36.305 5653 5655 5656 W 3749 40251 0.06% 0.011%

136 36.611 5705 5707 5710 W 3317 48270 0.07% 0.013% 137 37.451 5847 5850 5856 W 3 3048 73777 0.11% 0.020%

08265.D 041702SCAN.M Thu Apr 18 09:58:13 2002 Page 3

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