GCMS analysis results, Sample AE08265, April 22, 2002

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•3 8 10.083 1190 1192 1194 W 3 3069 36578 0.05% 0.010% 39 10.312 1228 1231 1234 W 4 3131 50927 0.08% 0.014% 40 10.424 1244 1250 1266 W 6 4222 159006 0.24% 0.044%

41 10.659 1282 1290 1294 W 4 2540 65944 0.10% 0.018% 42 11.452 1423 1425 1427 W 2108 20607 0.03% 0.006% 43 11.587 1444 1448 1451 PV 2078 27753 0.04% 0.008% 44 11.616 1451 1453 1457 W 3 1805 24255 0.04% 0.007% 45 11.910 1499 1503 1506 W 3 3570 58290 0.09% 0.016%

46 11.986 1510 1516 1523 W 2 2138 69338 0.10% 0.019% 47 12.080 1527 1532 1538 W 3 3293 80891 0.12% 0.022% 48 12.404 1583 1587 1591 PV 3 2044 32477 0.05% 0.009% 49 12.457 1591 1596 1606 W 31684 517585 0.77% 0.143% 50 12.568 1611 1615 1623 W 3 3788 72321 0.11% 0.020%

51 12.756 1642 1647 1657 W 4 3689 99282 0.15% 0.027% 52 13.485 1760 1771 1788 W 3226295 59409152 88.89% 16.388% 53 13.632 1788 1796 1808 W 3 10366 268956 0.40% 0.074% 54 13.873 1834 1837 1843 W 2 3461 71729 0.11% 0.020% 55 14.090 1869 1874 1882 W 3 2463 58646 0.09% 0.016%

56 14.301 1897 1910 1916 W 5 3582 93072 0.14% 0.026% 57 14.660 1965 1971 1975 W 4 2447 48101 0.07% 0.013% 58 15.747 2152 2156 2161 W 3 4095 71637 0.11% 0.020% 59 15.94 7 2187 2190 2196 W 5 3178 55687 0.08% 0.015% 60 16.434 2259 2273 2286 W 3 2852 104002 0.16% 0.029%

61 16.804 2330 2336 2347 W 4 6682 144754 0.22% 0.040% 62 17.175 2390 2399 2401 W 3 2290 41637 0.06% 0.011% 63 17.210 2401 2405 2409 W 2 2251 28509 0.04% 0.008% 64 17.457 2441 2447 2452 W 5 2488 45530 0.07% 0.013% 65 18.632 2632 2647 2669 PV 3379137 65732634 98.35% 18.132%

66 18.773 2669 2671 2673 W 2 2359 30174 0.05% 0.008% 67 18.873 2681 2688 2697 W 5 5223 119396 0.18% 0.033% 68 19.020 2710 2713 2729 W 5 3023 83418 0.12% 0.023% 69 19.249 2749 2752 2760 W 3 1697 32587 0.05% 0.009% 70 19.842 2849 2853 2858 PV 3 1820 27424 .0.04% 0.008%

71 20.206 2904 2915 2929 PV 6 2692 90023 0.13% 0.025% 72 20.389 2929 2946 2952 W 3 19212 358626 0.54% 0.099% 73 20.430 2952 2953 2959 W 2 1906 22767 0.03% 0.006% 74 20.600 2971 2982 2997 W 331977 6019457 9.01% 1.660% 75 20.941 3037 3040 3042 W 1487 16150 0.02% 0.004%

76 21.058 3050 3060 3067 W 5 4784 153410 0.23% 0.042% 77 21.ill 3067 3069 3077 W 3 2637 46237 0.07% 0.013% 78 21.211 3077 3086 3092 W 4 2290 64469 0.10% 0.018% 79 21.258 3092 3094 3097 W 2 2384 37101 0.06% 0.010% 80 21.299 3097 3101 3107 W 4 3112 63944 0.10% 0.018%

81 21.458 3124 3128 3134 W 3 2935 61439 0.09% 0.017% 82 21.611 3150 3154 3163 W 5 1910 57376 0.09% 0.016% 83 21.722 3168 3173 3175 PV 2 1808 20357 0.03% 0.006% 84 21.822 3181 3190 3195 W 2 24765 455760 0.68% 0.126% 85 21.863 3195 3197 3205 W 4 7694 159799 0.24% 0.044%

86 22.069 3226 3232 3236 W 4 1694 38074 0.06% 0.011% 87 22.104 3236 3238 3240 W 2 2019 13576 0.02% 0.004%

08265.D 041702SCAN.M Thu Apr 18 09:58:13 2002 Page 2

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