GCMS analysis results, Sample AE08262, April 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020417\08262.D Vial: 19 Acq On : 18 Apr 2002 12:18 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 Methylene Chloride Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

4.04 0.27 ug/L 264555 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methylene Chloride 84 CH2C12 000075-09-2 2 2 Borane, trifluoro- 68 BF3 007637-07-2 1 3 Ethanol, 2,2-dichloro- 114 C2H4C12O 000598-38-9 1 4 Methylene Chloride 84 CH2C12 000075-09-2 1 Abundance Scan 164 (4 043 min): 08262 D (-156) (-) m/z 49.00 100.00% 49 38 85 5000

3.60 3 80 4 00 4 20 4.40 0 ■ 1 । 1 1 ' ' । ■ 1 i ■ ■ । l ■ • l । ■ ■ ■ ' i ■ ■ ■ ■ i ■ ■ • ' । >1 m/z 38.00 54.68% m/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #111041: Methylene Chloride 49

84 5000 (1 PTgi ■ Ta l /I l e 3 60 3 80 4 00 4 20 4.40 m/z 85.00 49.85%

n/z-> 0- 0 29 41 1 1 I 1 1 1 ' I ' ' tI’i 1 1 1 ' I1''1 10 20 30 40 14—— 50 59 65 73 ■‘l ’''Ip' ■ ' l ' 60 70 80 90 ' '100 ' ' 110 ' ' 120 Abundance #12321 Borane, trifluoro- 49 i, mrapoonmup™ ppr ■, TP 3 60 3.80 4 00 4 20 4 40 5000- m/z 87.90 41.39%

68 m/z—> 0- 0 119 10 20 3030 . 3840 . 50 60 70 80 90 100 110 120 ABd"MHApMwMayn MW Abundance #1082 Ethanol, 2,2-dichloro- 31 3.60 3.80 4.00 4 20 440 m/z 41.00 31.72%

5000 I

25 , 37 43 49 55 61 70 77 83 96 103 114 0- ‘I8 ‘ r-ttr I ' I'1' Il......................... 1 'T1'1'' । i '1 1 । i 1 ■ ■ 1 । ■ 1 1 ■ i ■ ■ n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 3.60 3 80 4 00 4.20 4.40

08262.D 041702SCAN.M Thu Apr 18 09:49:31 2002 Page 8

NYC-WTC_000048320