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GCMS analysis results for sample AE08429, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08429 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048207–000048219

Folder label: “GCMS X 4/9/02 A 4/19/02

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Scanned page image, NYC-WTC_000048209
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020419\08429.D Vial: 16 Acq On : 19 Apr 2002 10:54 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 26 14:51:19 2002 Quant Results File: SCAN020418.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Mon Apr 22 08:00:39 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 10815323 40.00 ug/1 -0.05 10) Naphthalene-d8 ' 16.54 136 41607140 40.00 ug/1 -0.07 17) Acenaphthene-dl0 24.46 164 22893968 40.00 ug/1 -0.06 30) Phenanthrehe-dlO 31.72 188 34289348 40.00 ug/1 -0.06 38) Chrysene-dl2 39.94 240 26336914 40.00 ug/1 -0.07 44) Perylene-dl2 43.16 264 18921223 40.00 ug/1 -0.04 System Monitoring Compounds 27) TCMX 27.54 207 823333 5.79 ug/1 -0.07 Spiked Amount 10.000 Recovery = 57.90% Target Compounds .o 72. Qvalue 35) Di-n-butylphthalate 34.81 149 101442 0.08 ug/1 97 36) Fluoranthene 36.05 202 127792 0.13 ug/1 80 39) Pyrene 36.66 202 86325 0.08 ug/1 81

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08429.D SCAN020418.M Fri Apr 26 15:04:00 2002 Page 1

NYC-WTC_000048209

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NYC-WTC_000048209Source: NYC Law Department, mirrored locally

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