GCMS results sample AE05749, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR1702\5749.D Vial: 19 Acq On : 18 Apr 2002 1:47 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 9 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

45.41 15.26 ug/1 1560080 Perylene-dl2 37.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3 -Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 2 dl-Xylitol, cyclic/2,3 -(phenylboron 238 C11H15BO5 074793-46-7 27 3 N-Benzhydrylidene-i- (2,4,6-trimethy 343 C24H25NO 089839-57-6 27 4 Ethanedioic acid,/bis(trimethylsily 234 C8H1804Si2 018294-04-7 16 Abundance Scan 4397 (45.408 min): 5749.D (-) m/z 73.00 100.00% 73 147 221

5000 281 355 429 45.00 45.20 45.40 45.60 45.80 45 1 1 i ■ 1 .117—— —tre ,1 251, , I 3271 401 - 191 ' I 1 ' ' T ' 11 r I1' iiti m/z 147.00 78.46% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 Dkid.B I | I I i । | । i r i" ] i i I I | | I

147 45.00 45.20 45.40 45.60 45.80 m/z 221.05 72.27% 221 281 397 A4E _.... ... 327,......415........ 519 561 1 I ' f ' ' I ' ' r' I ' ' 1 1 I............. ... 1................. , . , I , , m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #31417: dl-Xylitol, cyclic 2,3-(phenylboronate) 147

45.00 45.20 45.40 45.60 45.80 61 5000 m/z 281.00 37.77% 104 31 177

I ।207 238 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #48514: N-Benzhydrylidene-1 -(2,4,6-trimethylphenyl)ethylami 147 45.00 45.20 45.40 45.60 45.80 m/z 355.05 34.75% 5000

, 182 312 343 T* । । । । । । mlz-> 50 100 150 200 250 300 350 400 450 500 550 45.00 45.20 45.40 45.60 45.80

5749.D GCMS0412.M Thu Apr 18 14:10:41 2002 Page 9

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