GCMS results sample AE08257, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08257.D Vial: 15 Acq On 17 Apr 2002 9:01 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 3 Guanidine Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

6.03 0.21 ug/L 220107 1,4-Dichlorobenzene-d4 9.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Guanidine 59 CH5N3 000113-00-8 5 2 Guanidine 59 CH5N3 000113-00-8 5 3 Diacetamide 101 C4H7NO2 000625-77-4 5 4 Acetamide 59 C2H5NO 000060-35-5 4 Abundance Scan 503 (6,035 min): 08257.D (-501) (-) m/ z 59.10 100.00% 43 53

/

5000-

84 101

5.60 5.80 6.00 4 1—LI 6 20 6 40 - 04 TT I " '■ I I " ‘' I " " I TTTTTTTTTTTTTTTTTTTTTTTTTTT m/ z 43.05 84.21% n/z- > 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #109753 Guanidine 43 59

5000- 5 60 5 80 6 00 6 20 6 40 m/z 101.10 42.37% 28 ■I pirm n irpllt |I . np ii i |I 0+ I....... ....... I’’A’I’’’L’S’l’’+’’J’IIIITITI* n/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #19412 Guanidine 43 59 5 60 5 80 6 00 6 20 6.40 5000 m/z 58.10 41.71%

n/z-> Abundance 0- mlm ......... 28 I " 1'i " " i " ‘' i " " i'1'' r " 11' " 111" 111" 11 "1111 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110

43 #5859: Diacetamide 5.60 m/ z 5.80 MMyo 6.00 4 6.95 6 20 6.40 12.76% 5000- 59 73

101

n/z-> 0- 23 28 38 ,| । 54 TTHNT TIHT 11''1' 11 79 -67—— 86 92 1. 11" " i'1" r " ' r " 111" ' i'11 ■ i " ■ ■ i " 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 5 60 580 600 6 20 6 40

08257.D 041702SCAN.M Thu Apr 18 09:33:55 2002 Page 8

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