GCMS results for sample AE07766, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020415\07766.D Vial: 28 Acq On 16 Apr 2002 8:51 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 1,4-Butanediamine Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 3.77 0.23 ug/L 148495 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Butanediamine 88 C4H12N2 000110-60-1 3 2 1,3-Dioxolan-2-one 88 C3H403 000096-49-1 2 3 Propanoic acid, 2-methyl- 88 C4H802 000079-31-2 2 4 1,3 -Dioxolan-2-one 88 C3H403 000096-49-1 2 Abundance Scan 117 (3 767 min): 07766 D (-110) (-) m/z 43.30 100.00% 43

5000

40 MA NAw, Im, m.A, 48 88 340 3.60 3.80 4.00 4.20

Tl/Z-> 01 Trpn-TTpn-rTp-rTTYrrTTp^ 5 10 15 20 25 30 5.1, -H— mTT 35 40 45 50 55 60 65 70 75 80 85 90 95 m/z AtyWWWWWW 40.20 16.34% Abundance #739 1,4-Butanediamine 35

5000 43 3.40 3 60 ' 3 80 4 66 4 20 m/z 41.20 15.64% ,18 97 59 0+ 1215 I 1 ... 39111 .. , 52 56 p-T rt jtll . | I i . ■ | I 111 6770 7 6 79 84 88 15" 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 11111111 ' i1 r'11'' " r ■ " i1" ' i ‘ ■111" ■ ■ i " n/z-> Abundance #108060: 1,3-Dioxolan- 2-one A 29

' i 1 ' I ' ‘ 1 ' I r ' I1 3.40 3 60 3.80 4 00 4 20 43 m/ % z 44.20 9.11% 5000- 88

58 0+ .. pil PPT 5" 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 BOMB ' i1' " i1 " 111' 11 ■ n/z-> Abundance #109340 Propanoic acid, 2-methyl- 43 3.40 3 60 380 4.00 4 20 m/z 88.10 8.17% 5000- 27 73 39 88 55 6 0 69 /z— > 1518 0 TTTTTTTUTTTTTT ....... .... 5 10 15 20 25 30 47 76 84 I '1'I' ■1'I''' 'I ।' ” 11' "T " 11 " " I " 1' 1 " 111111 35 40 45 50 55 60 65 70 75 80 85 90 95 3.40 441/71/0101—91 3 60 3 80 4 00 4.20

07766.D 041202SCAN.M Tue Apr 16 13:41:58 2002 Page 4

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