GCMS results sample AE08255, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08255.D Vial: 13 Acq On 17 Apr 2002 7:22 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: l. 00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L Peak Number 7 Hydantoin Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 9.75 0.30 ug/L 317517 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydantoin 100 C3H4N202 000461-72-3 4 2 2-Butenoic acid, 4-oxo- 100 C4H403 022418-77-5 3 3 Ethanedial 58 C2H202 000107-22-2 3 4 Ethene, methoxy- 58 C3H60 000107-25-5 3 Abundance Scan 1136 (9 754 min): 08255.D (-1134) (-) m/z 40.00 100.00% 40

5000 58 100 117 9.40 9.60 9.80 10.00

s 87 01 .|i .। m/z 58.10 28.61% n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #116 Hydantoin 28 100 Pyyn 5000 i 1 ' 1 ■ i 1 72 9 40 9 60 9.80 10 00 43 m/z 57.30 26.05% 57 0+ 14 H ... il, 54.. 82 n/z-> Abundance ' i 1 1 1 1 i ■ 10 20 30 40 50 60 70 #62: 2-Butenoic acid, 4-0x0- 8” 90 100 110 120

27 55 —4 r 4 . 940 960 9.80 10.00 5000 100 m/z 117.00 25.30% 45 72

37 83 _

n/z-> 01 ‘ । ■1 ' ■ । 10 20 ■ 30 40 50 4— 60 65-— 70 80 90 100 110 120 Abundance Ethanedial ................................/ ............. 23 940 9.60 9.80 10.00 m/z 99.90 25.15% 5000 58

44

/z- > 0 15 ''i'241I [35,414774.,,. ......... 10 20 30 40 50 60 70 80 90 100 110 120 9 40 9 60 14,49 80 10 00

08255.D 041702SCAN.M Thu Apr 18 09:24:58 2002 Page 11

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