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GCMS analysis results for sample AE08253, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08253 conducted on April 19, 2002, including surrogate recovery data.

NYC-WTC_000047830–000047850

Folder label: “GCMS X 4/8/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08253.D Vial: 11 Acq On : 17 Apr 2002 5:42 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Pentasiloxane, dodecamethyl- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

35.51 0.25 ug/L 270391 Perylene-dl2 34.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentasiloxane, dodecamethyl- 384 C12H3604Si5 000141-63-9 17 2 2-Amino-2-oxo-acetic acid, N-[3,... 221 C12H15NO3 1000127-85-3 5 3 1H-Indole-2,3-dione, 5-chloro-l-... 282 C12H15ClN2O2Si 1000143-06-1 4 4 2H-Indazol-3-amine, 2-methyl- 147 C8H9N3 1000142-18-7 4 Abundance Scan 5520 (35.512 min). 08253.D (-5508) (-) m/ z 73.05 100.00% 40 73 /I 147 221 5000 281 355 429 35.20 35.40 35.60 35.80 0 1 1i 1 ' I ' ' 1 m/ z 40.00 89.83% m/z-> 50 100 150 200 250 300 350 400 Abundance #115143: Pentasiloxane, dodecamethyl- 73 147 281

5000 i ■ ■ ■ 1 i 369 35.20 35.40 35.60 35.80 207 m/z 147.00 66.93% 93100117 ,’ ' 177,1 r 249 45 0- 1 hr + , 1 1 1 'T ' 1 —1 1 — ----- 1 1 ' m/z-> 50 150 200 250 300 350 400 Abundance #87891: 2-Amino-2-oxo-acetic acid, N-[3,4-dimethylphenyl]-... 221 1).. ... 35.20 35.40 35.60 35.80 147 5000 120 m/z 221.10 63.75%

77 01 . 51 | 104 ii__ 174193 1 l , !-I T | . "ka ' 11 1 1 ' m/z-> 50 100 150 200 250 300 350 400 Abundance #27596: 1H-lndole-2,3-dione, 5-chloro-1-(trimethylsilyl)-,... 1 1 1 1 1 ' 1 1 1 1 1 I 73 35.20 35.40 35.60 35.80 m/z 2 07.00 35.72%

5000 45 251

282 Mqpupoda/MPww - 1 EO 196 । 0 93 115 117 0 ,4216.1 1,4 TT1 k kl I-1 1 1 । । । ' > । । [ । । । > । । । । । “j' । i11 Ip /z-> 50 100 150 200 250 300 350 400 35.20 35.40 35.60 35.80

08253.D 041702SCAN.M Fri Apr 19 08:38:12 2002 Page 15

NYC-WTC_000047848

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NYC-WTC_000047848Source: NYC Law Department, mirrored locally

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