GCMS results for sample AE08068, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \MSDCHEM\1\DATA\020415\08068.D Vial: 25 Acq On : 16 Apr 2002 6:25 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 14 Butanamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.07 130.09 ug/L 85648300 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butanamide 87 C4H9NO 000541-35-5 38 2 3-Pentanol 88 C5H120 000584-02-1 36 3 2-Pentanol, 2-methyl- 102 C6H140 000590-36-3 36 4 2-Propanol, 2-methyl -______________ 74 C4H10O 000075-65-0 33 Abundance Scan 679 (7,069 min): 08068 D (-664) (-) m/ z 59.30 100.00% 59

5000- 43

69 - 151 6 80 7 00 7 20 7 40 0 36, "1‘1Yf1151 || 80 8/ 95 107 121 136 || m/z 43.25 3 6.61% . (II TTT 11 ''1 11' ''' i'' '' i'1'' i1 11 ' i '1111 ■ '111' ' 111" ■ ■ i ■ ' TVz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #19496 Butanamide 59 44 5000 6.80 7.00 7 20 7 40

27 i 72 m/z 41.30 16.33% 15 87 0+ 1 ' i ■''' i ' ,____ I — ' ■ i ■ ■ Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #113150 3-Pentanol 59

6 80 700 7 20 7 .40 5000 31 m/z 151.20 10.01% 41

0+ "Iil 15 4 — 50——— 70 87 ■ i ' ■ 11 r ■ ■ ■ i' n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #113241 2-Pentanol. 2-methy- 59 ....... .. ....... A. 6.80 7.00 7 20 7 40 m/z 153.20 9.59% 5000 45 87

n/z-> 0 31/ ■ i ■ ■ ■ • i • • ■ 11 ■ 10 20 30 H 69 ■ ■ i ■ • ■ ’ i ■ 40 50 60 70 80 90 100 110 120 130 140 150 160 6.80 7.00 7 20 7 40 '

08068.D 041202SCAN.M Tue Apr 16 13:56:53 2002 Page 17

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