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GCMS calibration results for sample AE07978, April 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS calibration analysis for sample AE07978 conducted between April 5 and 15, 2002, listing compound responses.

NYC-WTC_000046695–000046698

Folder label: “GCMS X 4/5/02 A 4/16/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\1\DATA\020415\0415C3.D Vial: 2 Acq On 15 Apr 2002 11:25 am Operator: Nefliu Sample ccv Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 16 11:02:19 2002 Quant Results File: 041202SCAN.RE

Quant Method : C: \MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Tue Apr 16 11:02:14 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.63 202 31224927 49.62 ug/L 100 38) Pyrene 27.27 202 32390271 48.81 ug/L 100 39) Butylbenzylphthalate 29.61 149 13241179 50.73 ug/L 100 40) Benzo(a)anthracene 30.87 228 28514318 57.51 ug/L 100 41) Bis(2-ethylhexyl)phthalate 31.47 149 17273486 52.63 ug/L 100 42) Chrysene 30.98 228 27553309 58.11 ug/L 100 44) Di-n-octylphthalate 33.33 149 26997786 47.25 ug/L 100 45) Benzo(b)fluoranthene 33.85 252 24652654 47.14 ug/L 100 46) Benzo(k)fluoranthene 33.93 252 26120006 45.60 ug/L 100 47) Benzo(a)pyrene 34.65 252 21865304m 57.76 ug/L 48) Indeno(1,2,3-cd)pyrene 37.52 276 14387091 53.68 ug/L 100 49) Dibenz(a,h)anthracene 37.64 278 14384387 50.60 ug/L 100 50) Benzo(g,h,i)perylene 38.29 276 13488035 50.39 ug/L 100

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0415C3.D 041202SCAN.M Wed Apr 17 15:53:57 2002 Page 2

NYC-WTC_000046697

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NYC-WTC_000046697Source: NYC Law Department, mirrored locally

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