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GCMS analysis results for sample AE07313, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07313 conducted on April 10, 2002, including surrogate recovery data.

NYC-WTC_000046624–000046634

Folder label: “GCMS X 3/28/02 A 2/27/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\APR0302\7313.D Vial: 9 Acq On 3 Apr 2002 8:35 pm Operator: Sample gc/ms scan 3/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.215 342 345 351 rBV 155479 341494 9.81% 2.128% 2 8.280 351 352 368 rVB 27300 72895 2.09% 0.454% 3 12.245 779 784 797 rBV 972880 2357837 67.72% 14.691% 4 14.843 1062 1067 1074 rVB 99266 190513 5.47% 1.187% 5 15.881 1174 1180 1196 rBV 1457896 3022106 86.80% 18.830%

6 21.187 1752 1758 1774 rBV 1698270 3481836 100.00% 21.694% 7 23.326 1986 1991 1997 rVB 120798 231653 6.65% 1.443% 8 25.630 2236 2242 2253 rBV2 1513649 3210415 92.20% 20.003% 9 33.691 3113 3120 3132 rBV2 778152 1761104 50.58% 10.973% 10 33.902 3138 3143 3155 rVB 119085 266691 7.66% 1.662%

11 37.932 3573 3582 3597 rBV2 378550 1112889 31.96% 6.934%

Sum of corrected areas: 16049433

7313.D GCMS0403.M Tue Apr 09 13:08:05 2002

NYC-WTC_000046629

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NYC-WTC_000046629Source: NYC Law Department, mirrored locally

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