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GCMS analysis results for sample AE07312, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07312 conducted on April 10, 2002, including surrogate recovery data.

NYC-WTC_000046613–000046623

Folder label: “GCMS X 3/28/02 A 2/27/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\APR0302\7312.D Vial: 8 Acq On 3 Apr 2002 7:35 pm Operator: Sample gc/ms scan 3/28 Inst' : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.248 780 785 798 rVB 1033517 2406905 67.79% 14.842% 2 14.846 1063 1068 1074 rVB 188352 360894 10.16% 2.225% 3 15.884 1175 1181 1195 rBV 1506818 3104168 87.42% 19.141% 4 21.190 1753 1759 1780 rBV 1752955 3550677 100.00% 21.895% 5 23.329 1987 1992 1999 rVB 109378 221827 6.25% 1.368%

6 23.935 2051 2058 2062 rBV 20540 36342 1.02% 0.224% 7 25.633 2236 2243 2254 rBV 1579121 3261963 91.87% 20.114% 8 33.693 3114 3121 3138 rBV2 793081 1840257 51.83% 11.348% 9 33.905 3139 3144 3158 rVB 125445 276048 7.77% 1.702% 10 37.935 3575 3583 3602 rBV 382455 1158040 32.61% 7.141%

Sum of corrected areas: 16217121

7312.D GCMS0403.M Tue Apr 09 13:07:49 2002

NYC-WTC_000046618

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NYC-WTC_000046618Source: NYC Law Department, mirrored locally

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