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GCMS reference analysis results for sample AE07311, April 2002

Machine-extracted title · confidence 95%

Laboratory report presenting GCMS reference analysis for sample AE07311 conducted on April 3, 2002, with measured values and MDLs.

NYC-WTC_000046578–000046602

Folder label: “GCMS X 3/28/02 A 2/27/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\APR0302\1965.D Vial: 6 Acq On 3 Apr 2002 5:35 pm Operator: Sample re-extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.842 192 196 204 rBV 53565 119200 3.76% 0.819% 2 6.952 204 208 214 rBV 51821 113344 3.58% 0.779% 3 7.191 227 234 243 rVB3 19443 50195 1.58% 0.345% 4 12.249 779 785 799 rVB 905761 2202438 69.48% 15.129% 5 14.847 1061 1068 1073 rVB 57322 109094 3.44% 0.749%

6 15.885 1175 1181 1198 rBV 1352377 2813289 88.74% 19.326% 7 21.191 1752 1759 1769 rBV 1516171 3170094 100.00% 21.777% 8 23.330 1985 1992 1998 rVB 77511 158845 5.01% 1.091% 9 25.634 2236 2243 2254 rBV 1359502 2913166 91.90% 20.012% 10 33.685 3114 3120 3134 rBV2 716162 1641008 51.77% 11.273%

11 33.906 3139 3144 3152 rW 104872 219699 6.93% 1.509% 12 37.927 3573 3582 3598 rBV2 342020 1046924 33.03% 7.192%

Sum of corrected areas: 14557296

1965.D GCMS0403.M Tue Apr 09 13:07:21 2002

NYC-WTC_000046596

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NYC-WTC_000046596Source: NYC Law Department, mirrored locally

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