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GCMS analysis results for sample AE06424, April 23, 2002

Machine-extracted title · confidence 100%

GCMS laboratory report for sample AE06424 analyzed on April 23, 2002, by analyst DLV.

NYC-WTC_000048776–000048792

Folder label: “GCMS X 4/11/02 A 4/15/02

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Scanned page image, NYC-WTC_000048781
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\APR1202\6424.D Vial: 9 Acq On : 15 Apr 2002 3:54 pm Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.204 340 344 364 rBV 369377 858252 20.73% 4.041% 2 12.234 777 783 799 rBV 1140073 2791241 67.41% 13.141% 3 14.832 1061 1066 1073 rVB 71628 140752 3.40% 0.663% 4 15.869 1173 1179 1195 rBV 1636786 3580568 86.47% 16.857% 5 21.166 1750 1756 1770 rBV 1990499 4140625 100.00% 19.494% 6 23.305 1983 1989 1999 rVB 208482 413469 9.99% 1.947% 7 25.609 2233 2240 2251 rBV2 1884674 4078975 98.51% 19.204% 8 33.670 3110 3118 3138 rBV2 1288838 2977943 71.92% 14.020% 9 37.902 3569 3579 3596 rBV2 727724 2258949 54.56% 10.635%

Sum of corrected areas: 21240774 6424.D GCMS0412.M Tue Apr 16 15:41:06 2002

NYC-WTC_000048781

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NYC-WTC_000048781Source: NYC Law Department, mirrored locally

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