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← Document results/DEP Box 27/GCMS X 4/11/02 A 4/15/02
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GCMS analysis results for sample AE06413, April 23, 2002

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GCMS laboratory report for sample AE06413 analyzed on April 23, 2002, by analyst DLV.

NYC-WTC_000048758–000048775

Folder label: “GCMS X 4/11/02 A 4/15/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\APR1202\6413.D Vial: 8 Acq On : 15 Apr 2002 2:56 pm Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 .625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 8.202 340 344 373 rVB 300110 722002 19.86% 3.814% 2 12.232 777 783 800 rVB 1013355 2435937 67.02% 12.867% 3 14.830 1060 1066 1073 rVB 117408 227835 6.27% 1.203% 4 15.867 1173 1179 1197 rBV 1481596 3156512 86.85% 16.673% 5 21.164 1750 1756 1768 rBV 1707388 3634628 100.00% 19.199% 6 23.303 1980 1989 1997 rVB 145878 313026 8.61% 1.653% 7 25.608 2233 2240 2251 rBV2 1644091 3573255 98.31% 18.875% 8 25.754 2252 2256 2264 rVB 12275 36530 1.01% 0.193% 9 33.668 3108 3118 3138 rBV2 1187790 2739820 75.38% 14.472% 10 37.900 3571 3579 3604 rBV2 663545 2092074 57.56% 11.051%

Sum of corrected areas: 18931619 6413.D GCMS0412.M Tue Apr 16 15:40:51 2002

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NYC-WTC_000048763Source: NYC Law Department, mirrored locally

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