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GCMS reference analysis results for sample AE07311, April 2002

Machine-extracted title · confidence 95%

Laboratory report presenting GCMS reference analysis for sample AE07311 conducted on April 3, 2002, with measured values and MDLs.

NYC-WTC_000046578–000046602

Folder label: “GCMS X 3/28/02 A 2/27/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

‘ Data File : C:\HPCHEM\1\DATA\MAR1302\1965.D Vial: 3 Acq On : 13 Mar 2002 12:01 pm Operator: Sample : re-extraction Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.196 337 343 354 rBV 12673 45490 1.24% 0.229% 2 12.309 785 791 800 rVB 938734 2429204 66.34% 12.209% 3 15.935 1180 1186 1204 rBV 1561276 3278139 89.53% 16.476% 4 21.250 1758 1765 1782 rBV 1746034 3594431 98.16% 18.066% 5 25.693 2242 2249 2259 rBV2 1679161 3661678 100.00% 18.404%

6 30.770 2797 2802 2810 rVB 187758 368437 10.06% 1.852% 7 33.763 3119 3128 3146 rBV2 1510373 3485859 95.20% 17.520% 8 38.032 3583 3593 3612 rBV2 935057 3032865 82.83% 15.244%

Sum of corrected areas: 19896103

1965.D GCMS0208.M Wed Mar 27 11:56:26 2002

NYC-WTC_000046589

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NYC-WTC_000046589Source: NYC Law Department, mirrored locally

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