GCMS analysis page, sample AE01503, March 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File C:\HPCHEM\l\DATA\MAR2602\1503.D Vial: 22 Acq On 27 Mar 2002 6:32 am Operator: Sample re-extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest.Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12 .-246 779 784 801 rBV 1412435 3473614 68.89% 15.086% 2 14.844 1063 1067 1072 rVB 49331 95450 1.89% 0.415% 3 15.891 1174 1181 1199 rBV 2230884 4618564 91.60% 20.059% 4 21.197 1752 1759 1770 rBV 2444254 5042356 100.00% 21.900% 5 25.640 2236 2243 2254 rBV2 2221624 4652581 92.27% 20.207%

6 30.708 2790 2795 2801 rBV 300589 589115 11.68% 2.559% 7 33.701 3114 3121 3135 rBV2 1166207 2718831 53.92% 11.808% 8 37.942 3573 3583 3598 rBV 627375 1834317 36.38% 7.967%

Sum of corrected areas: 23024828

1503.D GCMS0308.M Fri Mar 29 11:33:27 2002 1

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