GCMS analysis results for sample AE10136, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020513\10136.D Vial: 22 Acq On : 14 May 2002 9:21 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C: \MSDCHEM\1\METHODS\SCAN020507 .M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 o-Chloroaniline Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.09 0.40 ug/1 32614 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 o-Chloroaniline 127 C6H6C1N 000095-51-2 22 2 Pyridine-2 -thiol -1 -oxide 127 C5H5NOS 1000134-19-4 14 3 1-Methyl/3-nitropyrazole 127 C4H5N3O2 054210-32-1 9 4 5-Methyl-1 -nitropyrazole 127 C4H5N3O2 031163-85-6 9 Abundance * Scan 342 (5.089 min): 10136.D (-335) (-) m/z 128.90 100.00% 129

5000 48 81 93 .. , W... , । 1 ‘ i . . . . i . . . . । ■ ■ . . Tvsrsm 4.80 5.00 5.20 5.40 36 118 TPTTTTTTTTT — ■ ■i । 11 ■ 173 m/z 127.00 81.92% 111' ‘ I " " I' “ 11'11'I'11‘11 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #57726: o-Chloroaniline 127

life 5000 ■ i i | r > i i | ii i I | i i i i । i iii-

4.80 5.00 5.20 5.40 65 92 m/z 48.00 34.50% 12 52 ..III. 73 84 ,| 100 110 28 39 ----- ■i rrHr’t’ । । 11 n-|Ti । । ।'' i'' ‘11' I I I I I I I I I I I I I 1 I I I I I 1 I 1 I I r I I

m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #57599: Pyridine-2-thiol-1-oxide 127 4.80 5.00 5.20 5.40 5000 m/z 130.90 20.76% 39 83 110 28 51 an 69

m/z~> TTTT —H4 17 95 +-+H44—— TT —H i111 ■ i । ‘1111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 + T‘

Abundance #57462: 1-Methyl-3-nitropyrazole 127 4.80 5.00 5.20 5.40 m/z 49.00 19.15%

5000

42 52 97 "AWMHy/tayhay 66 80 | 111 1111'1' I'11 TFTH | TT TPmmm 11•" ■ । ।■i■■■•। m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 4.80 5.00 5.20 5.40

10136.D SCAN020507.M Wed May 15 08:32:16 2002 Page 3

NYC-WTC_000046209