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GCMS sample analysis results for AE10698, May 20 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GC/MS analysis of sample AE10698 including surrogate recovery data in May 2002.

NYC-WTC_000045707–000045720

Folder label: “GCMS X 5/3/02 A 5/13/02

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NYC 9/11 Public Portal Document

'Data File : C:\MSDCHEM\1\DATA\020513\10698.D Vial: 9 Acq On : 13 May 2002 8:26 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Smoothing : ON Filtering: 5 Sampling : 1 Min Area: 0.7 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.649 92 97 104 rBV3 19958 30075 0.76% 0.140% 2 6.123 512 518 521 rBV 33880 60523 1.53% 0.281% 3 6.158 521 524 557 rVB 377720 764367 19.28% 3.546% 4 11.375 1401 1412 1435 rBV 1137215 2827091 71.32% 13.116% 5 16.534 2270 2290 2310 rBV 1380963 3552717 89.63% 16.483%

6 24.454 3623 3638 3657 rBV 1355517 3712516 93.66% 17.224% 7 27.539 4150 4163 4175 rBV4 181792 499236 12.60% 2.316% 8 28.356 4292 4302 4314 rBV4 9820 28519 0.72% 0.132% 9 31.094 4757 4768 4778 rVB3 10078 28560 0.72% 0.133% 10 31.717 4855 4874 4898 rBV2 1349841 3963697 100.00% 18.390%

11 31.952 4906 4914 4932 rVB4 12238 39096 0.99% 0.181% 12 32.199 4939 4956 4967 rVB4 8683 29263 0.74% 0.136% 13 39.931 6259 6272 6288 rBV2 1815704 3495337 88.18% 16.217% 14 43.151 6809 6820 6845 rBV2 1256115 2522828 63.65% 11.705%

Sum of corrected areas: 21553825

10698.D SCAN020507.M Wed May 15 08:33:40 2002 Page 1

NYC-WTC_000045711

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NYC-WTC_000045711Source: NYC Law Department, mirrored locally

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