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GCMS analysis results for sample AE09451, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09451 including surrogate recovery data conducted on May 15, 2002.

NYC-WTC_000045516–000045525

Folder label: “GCMS X 5/3/02 A 5/8/02

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Scanned page image, NYC-WTC_000045521
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\MAY0802\9451.D Vial: 11 Acq On 8 May 2002 8:21 pm Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.154 336 340 346 rBV 477754 962511 24.82% 4.894% 2 8.227 346 348 368 rVB 48581 162575 4.19% 0.827% 3 12.195 775 781 792 rBV 1194669 2736781 70.56% 13.915% 4 15.824 1171 1177 1191 rBV 1693546 3474748 89.59% 17.667% 5 21.129 1750 1756 1772 rBV 1796813 3878697 100.00% 19.720%

6 23.274 1981 1990 1998 rBV2 199216 438527 11.31% 2.230% 7 25.574 2235 2241 2251 rW2 1685934 3573338 92.13% 18.168% 8 33.638 3114 3121 3139 rBV 1066630 2457537 63.36% 12.495% 9 33.858 3139 3145 3156 rVB 81956 201319 5.19% 1.024% 10 37.862 3572 3582 3601 rBV2 614014 1782421 45.95% 9.062%

Sum of corrected areas: 19668454

9451.D GCMS0507.M Thu May 09 14:43:28 2002

NYC-WTC_000045521

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NYC-WTC_000045521Source: NYC Law Department, mirrored locally

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