GCMS calibration table for sample AE09449, May 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0202\9449.D Vial: 8 Acq On 2 May 2002 9:39 pm Operator : Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 3 8:31 2002 Quant Results File: GCMS0501.RES

Quant Method C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) * Title 209 625/TCLP calibration table Last Update Wed May 01 10:40:31 2002 Response via Initial Calibration DataAcq Meth GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 601421 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 2228389 40.00 ug/1 -0.02 17) Acenaphthene-dlO 21.14 164 1211767 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.58 188 1728055 40.00 ug/1 -0.01 38) Chrysene-dl2 33.65 240 1140519 40.00 ug/1 -0.02 44) Perylene-dl2 37.88 264 771189 40.00 ug/1 0.00

System Monitoring Compounds 28) TCMX 23.27 209 36504 6.19 ug/L -0.02 Spiked Amount 10.000 Recovery = 61.90%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(l-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.42 77 808 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.88 128 388 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.61 149 996 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.58 178 566 N.D.

(#) = qualifier out of range (m) = manual integration 9449.D GCMS0501,M Fri May 03 08:31:22 2002 Page 1

NYC-WTC_000045507