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← Document results/DEP Box 25/GCMS X 4/29/02 A 5/3/02
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GCMS blank analysis results for sample AE09329, May 7 2002

Machine-extracted title · confidence 100%

Laboratory report showing blank test results for various organic compounds on May 7, 2002.

NYC-WTC_000044559–000044571

Folder label: “GCMS X 4/29/02 A 5/3/02

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NYC 9/11 Public Portal Document OCCL1 MpUu RCUL —

Data File C : \MSDCHEM\ 1 \DATA\ 0 5 0 2 0 2 \ 0 4 2 9LB . D Vial : 6 Acq On 2 May 2002 3:38 pm Operator: Mclean Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 3-Penten-2-one, 4-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 5.01 0.62 ug/L 303097 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penten-2-one, 4-methyl- 98 C6H10O 000141-79-7 83 2 2-Pentene, 2,3-dimethyl- 98 C7H14 010574-37-5 80 3 2-Pentene, 3,4-dimethyl-, (Z)- 98 C7H14 004914-91-4 78 4 3-Penten-2-one, 4-methyl- 98 C6H10O 000141-79-7 78 Abundance Scan 329 (5.012 min): 0429LB.D (-321) (-) m/ z 83.10 100.00% 55 83

5000 98 43 .. I I I I I ■ I I > I I1I I I I I 1 [ I I ................... 36 ,| 4.60 4.80 5.00 5.20 5.40 ............ 11 ■ I 48 1 i ■ 1 1 ' ' i 1 ■ ' 1 i 1 1 1 1 i 1 ' ' 1 i 1 1 i 1 1 m/ z 55.10 87.13% m/z-> 10 20 30 40 50 60 70 80 90 100 Abundance #116425: 3-Penten-2-one, 4-methyl- 55 83

5000 43 [ II I I I I I I I I I I I I I I 1 1 I I I I

98 4.60 480 5.00 5.20 5.40 29 m/ z 98.10 49.65% 36 , 38 50 | , I I I II I I Illi I I -—1 I ' I I 62 67 I ' I I ' I I I I 77 I 1 ' [ I 1189.1 i 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 Abundance #32863: 2-Pentene, 2,3-dimethyl- 55 83 41 । 1 ' 1 i ■ 1 ■■ i 1 1 1 1 i 1 1 1 1 i 1 1 4.60 4.80 5.00 5.20 5.40 5000 m/z 4 3.10 36.29% 27 98 69 15

m/z-> I 1 I 1 1 I 1 1 1 10 20 1 -361 504 50 V 60 1‘1‘i‘t 1 1 i'1'! 1 +91 63J, . , 77 , 70 80 30 40 90 100 Abundance #116420: 2-Pentene, 3,4-dimethyl-, (Z)- 55 83 4.60 4.80 5.00 5.20 5.40 m/z 39.10 20.94% 41 5000 27 98

15 69 ....... ....... 1 1 i 1 1 1 1 i ■ 32—+ —+ 50 । 1. 63| + —IP— 77, 4-, . | 93 I ' 1 1........... .... ............ /z-> 10 20 30 40 50 60 70 80 90 100 4.60 4.80 5.00 5.20 5.40

0429LB.D 050102.M Mon May 06 10:58:31 2002 Page 4

NYC-WTC_000044565

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NYC-WTC_000044565Source: NYC Law Department, mirrored locally

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