Gas chromatography-mass spectrometry analysis report for sample AE06340, conducted May 3, 2002, identifying other unknown compounds.
NYC-WTC_000044526–000044540Folder label: “GCMS X 4/29/02 A 5/1/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050102\6340.D Vial: 16 Acq On 1 May 2002 9:55 pm Operator: Mclean Sample re-ext 4/29 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L
Peak Number 5 1-Hexanol, 2-ethyl- Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T. 10.26 0.52 ug/L 331109 1,4-Dichlorobenzene-d4 9.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1-Hexanol, 2-ethyl- 130 C8H180 000104-76-7 78 2 1-Hexanol, 2-ethyl- 130 C8H180 000104-76-778 3 1-Hexanol, 2-ethyl- 130 C8H180 000104-76-7 78 4 1-Hexanol, 2-ethyl- 130 C8H180 000104-76-7 53 Abundance Scan 1222 (10,259 min): 6340.D (-1217) (-) m/ z 57.10 100.00% 57
5000 41 70 A) 83 98 112 10.00 10.20 10.40 10.60 ....................... I ll , 1 i । । । । । । iiii j n i i । ■ । r 51. ' i ■ ' PT --- m/z 41.10 45.16% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #15889:1-Hexanol, 2-ethyl- 57
5000 _AMAAANA AAA । । 1 | ' r i i । i > | T [ III | | 1 | 41 10.00 10.20 10.40 10.60 29 70 83 m/z 43.15 36.51%
TTH +63—14 77 |..... T.... 112 15 /z-> 1 1 i ■ 10 ' ' i ■ 20 I, '' 'W '1 30 ' 51 50 40 80 90 100 110 120 60 70 ■'' ।1' ■ ■ ।'' ■11''1 ■ ।1'1' ।'
Abundance #112147:1-Hexanol, 2-ethyl- 57 WNMWa WWppAN 1 ' l l ! I I > I I I I I I I I I I 1
10.00 10.20 10.40 10.60 5000 41 m/z 55.10 30.08% 29 70 83
1 1 1 i 1 1 1 1 I 1 18 T i I | i I I I । I 111 | [ r ......... ......................... । .li 98 T I I I > I ] I I I'I ' I I I — I—i I I I I 112 •n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #112165:1-Hexanol, 2-ethyl- MA" 1 i ' i • ■ 57 10.00 10.20 10.40 10.60 m/z 70.10 23.22% 5000 41 70 83 29 9 112 m/z—> 1 I ' 10 15 ' I 1 1 1 1 1 1 ' 1 1 r1 20 30 40 514 50 +63+11,7711.111 70 6080 90। 100 110 120 ' ' 1 ‘ । ■ | I l .-!■[■ I I I | | I
10.00 10.20 10.40 10.60
6340.D 050102.M Thu May 02 12:25:13 2002 Page 8
NYC-WTC_000044537
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NYC-WTC_000044510
Report listing other unknown compounds and surrogate recovery data from GCMS analysis conducted on May 3 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044496
Report listing other unknown compounds and surrogate recovery data from GCMS analysis conducted on May 3 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044541
Laboratory report documenting GCMS analysis of sample AE06407 conducted on May 3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045155
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10307 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044926
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10199 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044994
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10204 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043938
Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043958
Laboratory report for sample AE09969 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044978
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10203 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025447
Laboratory report showing GCMS results for sample AE11421 analyzed on May 30, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024083
Laboratory report detailing GCMS analysis of sample AE10896 conducted on May 21, 2002, including surrogate recovery data.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024153
Document noting low recovery in GCMS scan of sample AE10205 and subsequent re-extraction yielding 85% recovery.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044430
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 29 and May 1, 2002.
Filed in the same folder
NYC-WTC_000044431
Fragment of a document containing unreadable text and partial headers from a DEP laboratory procedure.
Filed in the same folder
NYC-WTC_000044433
Gas chromatography-mass spectrometry blank analysis showing results below method detection limits for organic compounds.
Filed in the same folder
NYC-WTC_000044447
Instrument qualification report for DFTPP showing pass/fail status for mass spectral limits on April 30, 2002.
Filed in the same folder
NYC-WTC_000044449
Calibration data for GCMS analysis of volatile organic compounds recorded on May 2, 2002.
Filed in the same folder