GCMS reference analysis results for sample AE06337, May 3 2002

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’3 8 14.049 1864 1867 1878 PV 3 1385 12411 0.03% 0.005% 39 15.700 2142 2148 2156 PV 5 1881 50146 0.12% 0.021% 40 16.746 2322 2326 2331 PV 2 3367 65278 0.16% 0.027%

41 18.062 2547 2550 2552 W 1830 15335 0.04% 0.006% 42 18.244 2576 2581 2585 PV 2 2497 45336 0.11% 0.019% 43 18.573 2623 2637 2654 W 2166842 41913871 100.00% 17.502% 44 18.685 2654 2656 2658 W 2 2569 28818 0.07% 0.012% 45 18.973 2697 2705 2709 W 5 2174 63680 0.15% 0.027%

46 20.541 2962 2972 2983 W 288552 5090701 12.15% 2.126% 47 20.688 2994 2997 3009 W 3 2741 61200 0.15% 0.026% 48 21.769 3177 3181 3186 PV 3 2083 39982 0.10% 0.017% 49 22.580 3312 3319 3326 BV 2 18263 323114 0.77% 0.135% 50 22.962 3371 3384 3403 PV 2 1892202 41453696 98.90% 17.310%

51 23.109 3403 3409 3432 W 3 25722 811209 1.94% 0.339% 52 25.089 3738 3746 3752 PV 3 1145 29245 0.07% 0.012% 53 28.802 4368 4378 4380 PV 2 1657 34476 0.08% 0.014% 54 29.484 4486 4494 4500 PV 1733 37296 0.09% 0.016% 55 29.983 4572 4579 4580 PV 3 633 7344 0.02% 0.003%

56 30.818 4709 4721 4762 PV 2 1525523 37841720 90.28% 15.802% . 57 31.082 4762 4766 4770 W 3 2700 60388 0.14% 0.025% 58 31.394 4810 4819 4842 PV 3 41565 1668069 3.98% 0.697% 59 31.540 4842 4844 4852 W 6 4302 100247 0.24% 0.042% 60 31.599 4852 4854 4857 W 2196 23270 0.06% 0.010%

61 34.719 5372 5385 5419 W 2 1169884 31013487 73.99% 12.951% 62 34.931 5419 5421 5425 W 2 5994 96220 0.23% 0.040% 63 34.960 5425 5426 5431 W 5 4326 86528 0.21% 0.036% 64 35.219 5468 5470 5474 W 3 1819 24078 0.06% 0.010% 65 35.542 5519 5525 5527 W 2 2013 28099 0.07% 0.012%

66 36.494 5680 5687 5698 W 3 2217 85021 0.20% 0.036% 67 36.828 5737 5744 5747 W 3 1989 44613 0.11% 0.019% 68 37.122 5790 5794 5800 PV 2 2114 32461 0.08% 0.014% 69 39.420 6183 6185 6189 W 3 1929 19624 0.05% 0.008%

Sum of corrected areas: 239474714

6337.D 050102.M Thu May 02 12:22:10 2002 Page 2

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