GCMS reference analysis results for sample AE06337, May 3 2002

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LSC Area Percent Report

Data File C:\MSDCHEM\1\DATA\050102\6337.D Vial: 13 Acq On 1 May 2002 7:29 pm Operator: Mclean Sample re-ext 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.144 4 11 21 BV 4975 84059 0.20% 0.035% 2 3.379 47 51 56 W 2 11656 156687 0.37% 0.065% 3 3.426 56 59 67 W 4 3280 41681 0.10% 0.017% 4 3.567 77 83 91 PV 8 2711 60196 0.14% 0.025% 5 3.649 91 97 106 PV 13818 242711 0.58% 0.101%

6 3.731 106 111 113 W 4 3200 58778 0.14% 0.025% 7 3.772 113 118 130 W 3 5359 135153 0.32% 0.056% 8 4.066 164 168 173 W 6 2490 40787 0.10% 0.017% 9 4.289 200 206 211 PV 4 3106 58920 0.14% 0.025% 10 4.372 211 220 226 W 6 3981 95634 0.23% 0.040%

11 4.601 255 259 269 W 6 2488 56730 0.14% 0.024% 12 4.671 269 271 275 W 3 2015 22108 0.05% 0.009% 13 4.965 313 321 326 PV 2 5036 80377 0.19% 0.034% 14 5.036 329 333 340 W 3 7336 147896 0.35% 0.062% 15 5.118 344 347 352 W 3 3410 60261 0.14% 0.025%

16 5.371 387 390 393 W 2 1721 16493 0.04% 0.007% 17 5.429 393 400 407 W 6 1908 46287 0.11% 0.019% 18 5.547 414 420 425 W 6 1999 52047 0.12% 0.022% 19 5.617 425 432 435 W 4 3609 81395 0.19% 0.034% 20 5.653 435 438 449 W 4 3841 121574 0.29% 0.051%

21 5.976 483 493 507 W 453110 7671257 18.30% 3.203% 22 6.064 507 508 515 W 5 5111 92947 0.22% 0.039% 23 6.957 654 660 668 PV 4 1929 50069 0.12% 0.021% 24 7.733 787 792 803 PV 4 6596 151728 0.36% 0.063% 25 8.749 961 965 974 W 5 2941 61340 0.15% 0.026%

26 9.301 1056 1059 1065 W 4 2785 49976 0.12% 0.021% 27 9.607 1104 1111 1117 W 6 1757 48492 0.12% 0.020% 28 9.701 1122 1127 1139 W 7 3025 83904 0.20% 0.035% 29 9.942 1159 1168 1181 W 1580170 29010131 69.21% 12.114% 30 10.030 1181 1183 1186 W 2 2396 27878 0.07% 0.012%

31 10.382 1237 1243 1246 W 4 2444 49029 0.12% 0.020% 32 12.034 1521 1524 1531 W 3 2672 48517 0.12% 0.020% 33 12.533 1604 1609 1616 W 3 2489 50170 0.12% 0.021% 34 12.727 1636 1642 1662 W 6 1938 75374 0.18% 0.031% 35 13.438 1751 1763 1781 PV 2045291 38972145 92.98% 16.274%

36 13.585 1781 1788 1794 W 7297 143776 0.34% 0.060% 37 13.831 1826 1830 1833 W 2 2037 21243 0.05% 0.009%

6337.D 050102.M Thu May 02 12:22:10 2002 Page 1

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