GCMS analysis results for sample AE10134, May 8 2002

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Data File C : \MSDCHEM\1\DATA\050202\10134.D Vial : 26 Acq On 3 May 2002 9:42 am Operator: Mclean Sample 4/29 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 8 1-Hexanol, 2-ethyl- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

10.26 0.26 ug/L 141154 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Hexanol, 2-ethyl- 130 C8H180 000104-76-7 53 2 1-Hexanol, 2-ethyl- 130 C8H180 000104-76-7 42 3 3-Undecene, 6-methyl-, (E)- 168 C12H24 074630-52-7 28 4 1-Hexene, 4-methyl- 98 C7H14 003769-23-1 16 Abundance Scan 1222 (10.259 min): 10134.D (-1217) (-) m/z 57.20 100.00% 57

5000 41 83 70 --- 98 10.00 10.20 10.40 10.60

m/z—> '11111111 ‘111' ■ ■11 10 20 30 4491 70 80 90 100 110 120 130 140 150 160 170 1' '11' 111 40 50 60 m/z 41.20 33.90% Abundance #15889:1-Hexanol, 2-ethyl- 57

5000 Il 11 11 11 ill IH ... I 1 I ' ' ' 41 10.00 10.20 10.40 10.60 29 70 83 m/z 43.20 30.50%

m/z-> 10 15 <4 TT+ 20 30 4050 + 80 90 100 110 120 130 140 150r 1'1601 r 1111701 11’ 60 70 li 98 112 apHangumspoeg...... I AMWpupw/NooAo Abundance #112146:1-Hexanol, 2-ethyl- 57

10.00 10.20 10.40 10.60 41 m/z 55.10 29.92% 5000 29

70 83

m/z-> 11 ■ r '111' +4 10 20 HHH 30 40 50 60 70 +4 I. 98112... 80 90 100 110 120 130 140 150 160 170 Abundance #15901: 3-Undecene, 6-methyl-, (E)- 57 10.00 10.20 10.40 10.60 m/z 83.10 26.46%

5000 1 41

m/z-> 29

TTTii > I > > I1.1. 10 20 30 TT4 40 50 60 + 70

70 83 98 ,| 112 125 140 158 168 ■11 |’ ■111'111 ■1 ■ ■ i1'111'1111 ■ ‘' ■ i'111111 ■11111111■ 80 90 100 110 120 130 140 150 160 170 10.00 10.20 10.40 10.60

10134.D 050102.M Mon May 06 12:24:16 2002 Page 11

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